Azeotropic and Extractive distillation

For more info about our services contact : help@bestpfe.com

Table of contents

1 INTRODUCTION
1.1 BACKGROUND
1.2 AIM OF THE PROJECT
1.3 PROJECT OBJECTIVES
2 THEORY
2.1 PHASE EQUILIBRIUM
2.1.1 Ideal system
2.1.2 Non-ideal system
2.1.3 Relative volatility
2.2 DISTILLATION
2.2.1 Simple distillation
2.2.2 Fractional distillation
2.2.3 Continuous distillation
2.2.4 Batch distillation
2.2.5 Azeotropic and Extractive distillation
2.3 EQUIPMENT
2.3.1 Columns and packing materials
2.3.2 Reflux divider and reflux ratio
2.4 MCCABE THIELES GRAPHICAL METHOD
2.5 SHORT CUT METHOD
3 EXPERIMENTAL METHODOLOGY
3.1 INITIAL TESTS WITH BINARY SYSTEMS
3.1.1 Bubble cap column
3.1.2 Initial evaluation method
3.1.3 Random packed column
3.1.4 Sampling from the boiler using a tube and a syringe
3.1.5 Sampling in the boiler using an IR-probe
3.2 TEST WITH MULTICOMPONENT SYSTEMS
4 RESULT AND DISCUSSION
4.1 INSULATION OF THE EQUIPMENT
4.2 EQUILIBRATION TIME
4.3 DISTILLATION VELOCITY
4.4 SAMPLING
4.5 MEASUREMENT WITH IR
4.6 MCCABE THIELE GRAPHICAL METHOD
4.7 SHORTCUT METHOD
4.8 RELATIVE VOLATILITY COMPARISON OBSERVED AND LITERATURE
4.9 AZEOTROPES AND MULTICOMPONENT SYSTEMS
5 CONCLUSION
6 REFERENCES