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Table of contents
Remerciements
1 Overview of solid state NMR
1.1 Introduction
1.2 Dipolar spin interactions in solid state NMR
1.3 Basic experimental techniques: Magic-Angle Spinning (MAS) and Cross Polarization (CP)
1.4 Dipolar recoupling and decoupling
1.5 Sensitivity enhancement techniques
1.6 Introduction to internal dynamics in biomolecules
1.7 Heteronuclear Overhauser Effect in organic solids
1.8 References
2 Sensitivity enhancement and quantitative 1D & 2D 13C spectra
2.1 Introduction to quantitative solid state NMR
2.2 Results and discussion
2.2.1 Overcoming the T1 (13C) constraints
2.2.2 Revealing the sources of the heteronuclear Overhauser enhancement .
2.2.3 Promoting uniform enhancements with low-power PARIS irradiation
2.2.4 Conclusions
2.3 References
3 Site-specific heteronuclear Overhauser measurements in filamentous Pf1 macromolecular assembly
3.1 Introduction
3.2 Sample preparation
3.3 Results and discussion
3.3.1 Recording site-specific one- and two-dimensional 13C NOE spectra
3.3.2 Probing internal dynamics of methyl groups in Pf1
3.4 References
4 Probing the gel to liquid-crystalline phase transition and relevant conformational changes in liposomes by 13C magic-angle spinning NMR
4.1 Introduction
4.2 Materials and methods
4.3 Results and discussion
4.3.1 Probing trans-gauche conformational changes
4.3.2 Revealing chain melting temperature (Tm)
4.3.3 Conclusions
4.4 References
5 Determination of sample temperature in unstable static fields by combining solid state 79Br and 13C NMR
5.1 Introduction
5.2 Materials and methods
5.3 Results and discussion
5.4 Conclusions
5.5 References
6 Sensitivity improvement during heteronuclear spin decoupling in solid-state NMR
6.1 Heteronuclear dipolar decoupling in solid state NMR
6.2 Experimental: NMR experiments and numerical simulations
6.3 Results and discussion
6.4 Conclusions
6.5 References
7 Effect of inherent rf field inhomogeneity on heteronuclear decoupling in solidstate NMR
7.1 Introduction
7.2 Experiments and numerical simulations
7.3 Results and discussion
7.4 Conclusions
7.5 References
