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Table of contents
Chapter 1. Literature survey of transparent and porous electrodes and their applications
1.1 Introduction
1.2. Preparation methods of the porous transparent conductive oxides
1.2.1. Non-templated particle deposition
1.2.2. Templated deposition
1.2.3. Physical deposition methods
1.2.4. Top-down methods
1.2.5. Electrospinning
1.3. Applications of the porous transparent conductive oxides
1.3.1. Energy generation and storage (photovoltaics, water splitting)
1.3.2. Electroanalysis
1.3.3. Other applications
1.4. Porous and transparent organic electrode materials
1.4. Conclusions
Chapter 2. Experimental
2.1. Chemicals
2.2. Preparation of the suspension
2.3. Preparation of indium tin oxide free-standing nanofiber mats
2.3.1. Electrospinning experiment
2.3.2. Post-treatment
2.3.3. Preparation of mats for measurements
2.4. Measurement procedures for indium tin oxide free-standing nanofiber mats
2.4.1. Electrochemical measurements
2.4.2. Spectroelectrochemical measurements
2.5. Preparation of indium tin oxide nanofilament layers
2.5.1. Substrate preparation
2.5.2. Electrospinning experiment and post-treatment
2.5.3. Mesostructured methylated silica deposition
2.5.4. Click-functionalized silica deposition and Ru complex functionalization
2.6. Measurement procedures for indium tin oxide nanofilament layers
2.6.1. Electrochemical measurements
2.6.2. Spectral measurements
2.6.3. Electrochemiluminescence measurements
2.7. Characterization
Chapter 3. Indium tin oxide free-standing nanofiber mats and their potential applications in electrochemistry and spectroelectrochemistry
3.1. Introduction
3.2. Results and discussion
3.2.1 Optimization of electrospinning
3.2.2. Electrochemical behavior of calcined ITO nanofibers
3.2.3. Thermal treatment of ITO nanofibers
3.2.4. Immobilization of the electrospun nanofibers with SnCl4
3.2.5. Application to the electrochemical detection of ascorbic acid
3.2.6. Application to spectroelectrochemistry
3.3. Conclusions
Chapter 4. Indium tin oxide nanofilament layers and their potential applications in electrochemistry and spectroelectrochemistry
4.1. Introduction
4.2. Results and discussion
4.2.1. Electrospun material characterization
4.2.2. Electrochemical properties of ITO nanofilaments
4.2.3. Electrochemical deposition of methylated silica
4.2.4. Electrochemical and spectral detection of industrial dyes
4.3. Conclusions
Chapter 5. Application of indium tin oxide nanofilaments in electrochemiluminescence generation
5.1. Introduction
5.2. Results and discussion
5.2.1. Electrochemiluminescence of dissolved Ru(bpy)32+
5.2.2. Electrochemiluminescence of adsorbed Ru(bpy)32+
5.2.3. Electrochemiluminescence of click-immobilized Ru(bpy)32+
5.2.4. Stability comparison between adsorbed and covalently bound luminophore
5.2.5. Possible explanations of the surprising phenomena
5.3. Conclusions
General conclusions and outlook
Conclusions générales et perspectives
Bibliography
