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Table of contents
1 Introduction
1.1 Overview
1.2 Intermetallic compounds in heterogeneous catalysis
1.3 Methanol steam reforming (MSR)
1.3.1 The reaction and its importance
1.3.2 Recent interest in M-Pd (M=Zn, Ga, In)
1.4 Other interest in In-Pd intermetallics
1.5 Surface alloys
1.5.1 Intermixing and segregation
1.5.2 In-Pd and similar systems: top-layer substitutional alloys
1.5.3 In-Pd and relevant systems: multilayer alloys and IMCs
1.6 Bulk In-Pd phases
1.6.1 Elemental palladium and indium
1.6.2 Discovery of the phases
1.6.3 In-rich Phases
1.6.4 Pd-rich Phases
1.6.5 InPd
1.7 Bulk IMC and alloy surfaces
1.8 Summary
2 Experimental Methods
2.1 Experimental Background
2.1.1 Experimental set-up
2.1.2 STM
2.1.3 LEED
2.1.4 XPS
2.1.5 Diamond Beamline I06
2.2 XPS data analysis
2.2.1 μXPS
2.2.2 Inelastic mean free path (IMFP) calculations
2.2.3 Quantifying in-house XPS data
2.2.4 Polycrystalline and bulk InPd surfaces
2.2.5 In/Pd(111) surface IMCs and alloys
3 Surface structures of In-Pd intermetallic compounds
3.1 Overview
3.2 Part I: Experimental study of In thin films on Pd(111) and alloy formation(Article)
3.3 Part II: Theoretical study of surface energies, alloying and segregationeffects (Article)
4 Bulk InPd IMC surfaces
4.1 Introduction
4.2 Growth of bulk InPd
4.2.1 InPd single crystals
4.2.2 Polycrystalline InPd
4.3 Single crystal InPd surfaces
4.3.1 Overview
4.3.2 InPd(100)
4.3.3 InPd(110)
4.3.4 InPd(111)
4.4 The polycrystalline surface
4.5 Discussion and Conclusion
5 Conclusion
A Pendry R-Factor
B LEED
Bibliography
